ZnS/ZrO2/graphene复合涂层制备及性能研究任务书

 2021-08-20 01:08

1. 毕业设计(论文)主要目标:

1、了解球磨工艺在纳米粉体制备方面的研究进展及相关领域的应用。2、掌握球磨工艺对纳米粉体粒径及形态结构的影响规律。3、掌握溶胶法及磁控溅射工艺在金属表面涂层制备制备的各影响因素。4、探讨ZnS/ZrO2/graphene的单一涂层结构与复合涂层结构的摩擦学行为。

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2. 毕业设计(论文)主要内容:

1.优化球磨工艺,获得不同粒径和形态的金属硫化物,氧化物及石墨烯复合结构。

2.研究溶胶旋涂及喷涂不同粒径及结构的复合涂层的表面质量及行为,通过接触角仪及粗糙度仪金星表面性能测试。

3.研究不同靶材磁控溅射后的复合涂层的表面质量及行为,通过接触角及粗糙度仪表面性能测试。

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3. 主要参考文献

[1]Baranowska-Korczyc, A., Reszka, A., Sobczak, K., Wojciechowski, T., Fronc, K. (2017). The synthesis, characterization and ZnS surface passivation of polycrystalline ZnO films obtained by the spin-coating method. Journal of Alloys and Compounds, 695, 1196-1204. [2]Mi, Y., Wang, J., Yang, Z., Wang, H., Wang, Z., Yang, S. (2014). Preparation and property of ZrO2/GO multi-layered nanocomposite lubricating film. RSC Adv., 4(75). [3]Mi, Y., Wang, Z., Liu, X., Yang, S., Wang, H., Ou, J., . . . Wang, J. (2012). A simple and feasible in-situ reduction route for preparation of graphene lubricant films applied to a variety of substrates. Journal of Materials Chemistry, 22(16). [4]Rana, A. u. H. S., Chang, S.-B., Chae, H. U., Kim, H.-S. (2017). Structural, optical, electrical and morphological properties of different concentration sol-gel ZnO seeds and consanguineous ZnO nanostructured growth dependence on seeds. Journal of Alloys and Compounds, 729, 571-582. [5]Rehman, Z. U., Heo, S. N., Cho, H. J., Koo, B. H. (2016). Vertically Aligned ZnO Nanorods: Effect of Synthesis Parameters. Journal of Nanoscience and Nanotechnology, 16(6), 6555-6559. [6]Zhou, Q., Huang, J., Wang, J., Yang, Z., Liu, S., Wang, Z., Yang, S. (2015). Preparation of a reduced graphene oxide/zirconia nanocomposite and its application as a novel lubricant oil additive. RSC Advances, 5(111), 91802-91812. [7]Zlotnikov, I., Gotman, I., Gutmanas, E. Y. (2008). Characterization and nanoindentation testing of thin ZrO2 films synthesized using layer-by-layer (LbL) deposited organic templates. Applied Surface Science, 255(5), 3447-3453.[8]李亚伟, 田彩兰, 赵雷, 李远兵, 金胜利, 李淑静. (2009). 碳包纳米氧化锆粉体的制备及其晶型转变.[J] 硅酸盐学报. 37(08), 1273-1276 1281. [9]By Aprillya Rosidian, Yanjing Liu, and RichardO. Claus.(1998).Ionic Self-Assembly of Ultrahard ZrO2/Polymer Nanocomposite Thin Films.Advanced Materials,1087-1091.[10]王金清, 刘晓红, 单小东, 杨生荣.(2004).ZrO2薄膜的力学性能和摩擦学性能研究.[J]材料科学与工程学报.22(5), 669-673.

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