固体酸催化剂制备脂肪酸甲酯任务书

 2021-10-06 12:10

1. 毕业设计（论文）的内容和要求

1. 查找阅读相关文献，了解课题背景，熟悉固体酸催化剂制备的基本原理，了解炭化、磺化反应过程中的各影响因素。

2. 掌握单因素分析的实验方法制备不同的固体酸催化剂。

3. 通过N2吸附脱附、XRD、TGA等进行催化剂表征分析。

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2. 参考文献

1. Chang, B.; Fu, J.; Tian, Y.etc. Soft-template synthesis of sulfonated mesoporous carbon with high catalytic activity for biodiesel production[J]. Rsc Advances 2013, 3 (6), 1987-1994.2. 方林; 张坤; 李晓红等, 磺酸基团功能化的碳-硅介孔复合材料的制备及其在生物柴油绿色合成中的应用[J]. Chinese Journal of Catalysis 2012, 33 (1).3. Samor, C.; Torri, C.; Fabbri, D, et al.Unusual Catalysts from Molasses: Synthesis, Properties and Application in Obtaining Biofuels from Algae[J]. ChemSusChem 2012, 5 (8), 1501-1512.4. Nakajima, K.; Hara, M., Amorphous Carbon with SO3H Groups as a Solid Brnsted Acid Catalyst[J]. ACS Catalysis 2012, 2 (7), 1296-1304.5. Lou, W. Y.; Guo, Q,et al. A Highly Active Bagasse‐Derived Solid Acid Catalyst with Properties Suitable for Production of Biodiesel[J]. ChemSusChem 2012, 5 (8), 1533-1541.6. Aldana-Prez, A.; Lartundo-Rojas, L.; Gmez, R, et al.Sulfonic groups anchored on mesoporous carbon Starbons-300 and its use for the esterification of oleic acid[J]. Fuel 2012.7. Rao, B.; Chandra Mouli, K.; Rambabu, N, et al.Carbon-based solid acid catalyst from de-oiled canola meal for biodiesel production[J]. Catalysis Communications 2011, 14 (1), 20-26.8. Fukuhara, K.; Nakajima, K.; Kitano, M, et al.Structure and Catalysis of Cellulose-Derived Amorphous Carbon Bearing SO3H Groups[J]. ChemSusChem 2011, 4 (6), 778-784.9. Zieba, A.; Drelinkiewicz, A.; Chmielarz, P, et al.Transesterification of triacetin with methanol on various solid acid catalysts: A role of catalyst properties[J]. Appl. Catal. A-Gen. 2010, 387 (1-2), 13-25.10. 周丽娜; 刘可; 华伟明等 碳基磺酸化固体酸材料的制备及其催化性能[J].催化学报 2009, 30 (3), 196-200.11. 乌日娜; 王同华; 修志龙等.生物质炭基固体酸催化剂的制备[J].催化学报 2009, 30 (12), 1204-1208.12. Lee, J.; Kim, J.; Hyeon, T., Recent progress in the synthesis of porous carbon materials[J]. Advanced materials 2006, 18 (16), 2073-2094.13. Toda, M.; Takagaki, A.; Okamura, M, et al.Default Green chemistry: Biodiesel made with sugar catalyst[J]. Nature 2005, 438, 178.14. Hara, M.; Yoshida, T.; Takagaki, A, et al. A carbon material as a strong protonic acid[J]. Angewandte Chemie International Edition 2004, 43 (22), 2955-2958.

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