1. 毕业设计（论文）的内容和要求
酸烯加成酯化过程无水生成，反应原子经济性高、工艺流程简单，是一种具有经济和环保双重优势的新型工艺，其关键在于绿色高效催化剂的开发。
目前酸烯酯化催化剂主要为固体超强酸、强酸性阳离子交换树脂、磺酸改性的介孔分子筛等。
为了抑制烯烃聚合提高羧酸酯的选择性，通常需要在反应体系中加入叔丁醇等极性溶剂或者使用大大过量的有机酸，这就导致后续产物分离能耗大或防腐蚀设备投资高等问题。
2. 参考文献
[1]项宗伟，乔旭 ，崔咪芬 ，汤吉海 ，陈献. 酸烯加成酯化制备丙烯酸叔丁酯的进展与研究[J]. 化工中间体，2010，4[2]赵崇峰, 程云, 王东, 等. 嗅化铜催化合成乙酸叔丁酯[J]. 辽宁石油化工大学学报, 2005, 25(2)[3]朱继芳, 廖世军. 羧酸/烯烃酯化合成羧酸酯工艺及催化剂研究进展[J]. 化学工业与工程, 1999, 16(5)[4]J Machado, J.E. Castanheiro, I. Matos,et al. SBA-15 with sulfonic acid groups as a Green Catalyst, for the acetoxylation of α-pinene[J]. Microporous nsted and Lewis acid sites[J]. Journal of Porous Materials, 2016, 23(1)[11]Kong L, Li F, Wang F, et al. In situ assembly of SiO2, nanodots/layered double hydroxide nanocomposite for the reinforcement of solution-polymerized butadiene styrene rubber/butadiene rubber[J]. Composites Science Technology, 2018, 158[12] Silva A R, Wilson K, Clark J H, et al. Covalent attachment of chiral manganese(III) salen, complexes onto functionalised hexagonal mesoporous silica and application to the asymmetric epoxidation of alkenes[J]. Microporous Mesoporous Materials, 2006, 91[13]Parry E P. An infrared study of pyridine adsorbed on acidic solids. Characterization of surface acidity[J]. Journal of Catalysis, 1963, 2(5)[14]Robinson K, Gibbs G V, Ribbe P H. The Structure of Zircon: A Comparison with Garnet[J]. American Mineralogist, 1971, 5-6[15] 王沛熹，姜冬梅.醋酸丁酯合成技术进展及市场趋势分析[J].精细化工原料及中间体，2005，（1)[16]Ballantine J A, Davies M, Purnell H, et al. Chemical conversions using sheet silicates: facile ester synthesis by direct addition of acids to alkenes[J]. Journal of the Chemical Society, Chemical Communications,1981,(1)[17]汤吉海，乔旭，周峰，等.一种羧酸和烯烃直接加成合成羧酸酯的方法[P].CN：102924272A，2013-02-13.[18] Trukhan N N, Romannikov V N, Shmakov A N, et al.H2O2-based selective oxidations over titaniumsilicates of SBA-15 type[J]. Microporous and mesoporous materials,2003,59(2)[19]田志茗，邓启刚，孙慧，等.对甲苯磺酸改性SBA-15的合成及催化合成乙酸正丁酯[J].应用化工，2007.36（8）[20]Yan Z, Tao S, Yin J, et al. Mesoporous silicas functionalized with a high density of carboxylate groups as efficient absorbents for the removal of basic dyestuffs[J]. Journal of Materials Chemistry,2006,16(24)
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