基于介孔氧化硅的温度响应型二氧化碳吸附剂的制备任务书

 2022-01-23 08:01

全文总字数:2773字

1. 毕业设计(论文)的内容和要求

毕业论文我们采用理论知识与实际实验操作相结合的方法设计一项实验,合成材料并检测其性能。

望同学认真完成以下相关任务:1,学会精确检索文献,并大量阅读相关文献,了解课题背景;2,熟悉实验原理和实验方法,设计实验路线;3,进行材料制备,并针对实验过程出现的问题对实验方案及时做出调整和改进;4,学习相关表征仪器如红外、核磁共振氢谱、热重、等的使用方法并对表征结果进行准确的分析;5,学习使用相关数据处理软件对数据进行分析与处理,根据实验结果进行总结;6,撰写论文,进行答辩。

2. 实验内容和要求

1,大量检索并阅读相关文献,了解课题背景及实验原理,设计实验方案;2,根据实验方案完成材料的制备;3,掌握相关表征仪器的操作,独立完成材料的表征以及性能测试;4,熟悉使用数据处理软件如origin,chemdraw,MestReNova对表征数据进行处理

3. 参考文献

Joos, Lennart, et al. "Carbon capture turned upside down: high-temperature adsorption Ethanol and MethanolEthanol Separations Using in Situ Confined Polymer Chains in a MetalOrganic Framework." ACS applied materials interfaces 11.44 (2019): 41383-41393.Hoshino, Yu, et al. "Reversible absorption of CO2 triggered by phase transition of amine-containing micro-and nanogel particles." Journal of the American Chemical Society 134.44 (2012): 18177-18180.Yue, Mengchen, et al. "Temperature‐responsive microgel films as reversible carbon dioxide absorbents in wet environment." Angewandte Chemie International Edition 53.10 (2014): 2654-2657.Werz, Patrick DL, Johannes Kainz, and Bernhard Rieger. "Thermo-and pH-responsive nanogel particles bearing secondary amine functionalities for reversible carbon dioxide capture and release." Macromolecules 48.18 (2015): 6433-6439.Seuring, Jan, et al. "Upper critical solution temperature of poly (N-acryloyl glycinamide) in water: a concealed property." Macromolecules 45.1 (2012): 374-384.Xu, Ziyang, and Wenguang Liu. "Poly (N-acryloyl glycinamide): a fascinating polymer that exhibits a range of properties from UCST to high-strength hydrogels." Chemical Communications 54.75 (2018): 10540-10553.Niskanen, Jukka, and Heikki Tenhu. "How to manipulate the upper critical solution temperature (UCST)?." Polymer Chemistry 8.1 (2017): 220-232.Liu, Fenglei, Wenhao Fu, and Shuixia Chen. "Synthesis, characterization and CO2 adsorption performance of a thermosensitive solid amine adsorbent." Journal of CO2 Utilization 31 (2019): 98-105.Chen, Yangguan, Guorong Lin, and Shuixia Chen. "Preparation of a Solid Amine Microspherical Adsorbent with High CO2 Adsorption Capacity." Langmuir 36.26 (2020): 7715-7723.Yoo, Chun-Jae, Pavithra Narayanan, and Christopher W. Jones. "Self-supported branched poly (ethyleneimine) materials for CO 2 adsorption from simulated flue gas." Journal of Materials Chemistry A 7.33 (2019): 19513-19521.Qiao, Shenglin, and Hao Wang. "Temperature-responsive polymers: Synthesis, properties, and biomedical applications." Nano Research 11.10 (2018): 5400-5423.

4. 毕业设计(论文)计划

2021.2.26-2021.3.10 查阅收集文献资料,了解课题背景,完成开题报告的撰写,为实验作准备工作2021.3.11-2021.3.31 根据实验方案进行相关材料合成2021.4.1-2021.4.15 对合成的样品进行相应的表征测试,并且撰写中期自查表2021.4.16-2021.4.30 探索吸附剂的吸附性能,同时撰写毕业论文。

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