全文总字数：6407字
1. 毕业设计（论文）的内容和要求
1、开题阶段。
搜集大量课题相关的文献，通过文献阅读了解微流场反应技术的发展现状以及硫叶立德的应用、传统合成方法及优缺点及电氧化偶联的机理理解。
凝练文献要点，形成文献综述。
2. 实验内容和要求
1、学习并掌握微流场反应、电催化技术的原理和一般操作过程，熟练掌握薄层层析色谱、柱层析分离等有机合成方法；2、筛选得到课题模板反应的最优条件；3、合成10-20个课题所需底物，并完成10-15个相应的底物扩增；4、通过核磁共振、质谱、单晶等分析方法确认所合成化合物的结构正确。
3. 参考文献
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Aggarwal, J. Am. Chem. Soc., 2010, 132, 1828-1830; (e) M.-M. Lou, H. Wang, L. Song, H.-Y. Liu, Z.-Q. Li, X.-S. Guo, F.-G. Zhang and B. Wang, J. Org. Chem., 2016, 81, 5915-5921; (f) Z.-W. Zhang, H.-B. Li, J. Li, C.-C. Wang, J. Feng, Y.-H. Yang and S. Liu, J. Org. Chem., 2020, 85, 537-547.3 (a) A.-H. Li, Y.-G. Zhou, L.-X. Dai, X.-L. Hou, L.-J. Xia and L. Lin, Angew. Chem., Int. Ed., 1997, 36, 1317-1319; (b) S. Hajra, S. M. Aziz, B. Jana, P. Mahish and D. Das, Org. Lett., 2016, 18, 532-535; (c) L. Li, M. Yang, Q. He and R. Fan, Nat. Commun., 2020, 11.4 (a) R. K. Kunz and D. W. C. MacMillan, J. Am. Chem. Soc., 2005, 127, 3240-3241; (b) Q.-Z. Li, X. Zhang, R. Zeng, Q.-S. Dai, Y. Liu, X.-D. Shen, H.-J. Leng, K.-C. Yang and J.-L. Li, Org. Lett., 2018, 20, 3700-3704; (c) D. Antoniak and M. Barbasiewicz, Org. Lett., 2019, 21, 9320-9325.5 (a) E. Vedejs, Acc. Chem. Res., 1984, 17, 358-364; (b) H. Zhang, B. Wang, H. Yi, Y. Zhang and J. Wang, Org. Lett., 2015, 17, 3322-3325; (c) I. Colomer, M. 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Oost, A. Oppedisano and N. Maulide, Chem. - Eur. J., 2020, 26, 10972-10975; (c) Y. Zhou, Y. Chen and Y. Huang, Org. Lett., 2020, 22, 5941-5946.9 (a) S. Kramer and T. Skrydstrup, Angew. Chem., Int. Ed., 2012, 51, 4681-4684; (b) J. Vaitla, A. Bayer and K. H. Hopmann, Angew. Chem., Int. Ed., 2018, 57, 16180-16184; (c) J. Lou, Q. Wang, Y.-G. Zhou and Z. Yu, Org. Lett., 2019, 21, 9217-9222; (d) S. Zhu, K. Shi, H. Zhu, Z.-K. Jia, X.-F. Xia, D. Wang and L.-H. Zou, Org. Lett., 2020, 22, 1504-1509; (e) Y.-X. Liang, M. Yang, B.-W. He and Y.-L. Zhao, Org. Lett., 2020, 22, 7640-7644.10 (a) S.-F. Zhu, Y. Cai, H.-X. Mao, J.-H. Xie and Q.-L. Zhou, Nat. Chem., 2010, 2, 546-551; (b) Z. Zhang, Y. Yu, F. Huang, X. Yi, Y. Xu, Y. He, J. B. Baell and H. Huang, Green Chem., 2020, 22, 1594-1604; (c) V. F. Batista, D. C. G. A. Pinto and A. M. S. Silva, ACS Catal., 2020, 10, 10096-10116; (d) Y. Li, Y.-T. Zhao, T. Zhou, M.-Q. Chen, Y.-P. Li, M.-Y. Huang, Z.-C. Xu, S.-F. Zhu and Q.-L. Zhou, J. Am. Chem. 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4. 毕业设计（论文）计划
2020.12.30-2021.1.31：毕业论文开题准备，撰写开题报告；2021.3.1-4.15：完成课题实验并整理数据；2021.4.16-2021.5.20：完成毕业论文撰写和论文答辩；2021.5.20-2021.5.25：毕业论文修订，整理。
以上是毕业论文任务书，课题毕业论文、开题报告、外文翻译、程序设计、图纸设计等资料可联系客服协助查找。
