电泳法制备四氧化三钴电极的研究任务书

 2022-01-18 08:01

全文总字数:3842字

1. 毕业设计(论文)的内容和要求

四氧化三钴是一种黑色固体,晶体结构为尖晶石构型,分子式为Co3O4。

它是一种混合价态的化合物,同时含有二价钴和三价钴。

它是重要的锂电池正极材料的原料,也可以直接用作锂电池的负极材料和超级电容器电极材料。

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2. 实验内容和要求

本课题以硝酸钴、柠檬酸为原料,采用水热反应合成前驱体,在100℃~200℃的温度下,利用高压反应釜水热反应不同时间后得到了四氧化三钴前驱体,再高温煅烧得到四氧化三钴。

将不同条件下制备得到的样品利用电泳法制备测试电极。

利用扫描电镜、紫外分光光度计等设备对电极进行表征。

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3. 参考文献

[1]Khalaj Maryam,Golkhatmi Sanaz Zarabi,Sedghi Arman. High-performance supercapacitor electrode materials based on chemical co-precipitation synthesis of nickel oxide (NiO)/cobalt oxide (Co3O4)-intercalated graphene nanosheets binary nanocomposites[J]. Diamond Findings from East China Normal University Broaden Understanding of Alloys and Compounds (Water Driven Photoluminescence Enhancement and Recovery of Ch3nh3pbbr3/silicon Oil/pdms-urea Composite)[J]. Chemicals Study Results from Banasthali Vidyapith in the Area of Energy Reported [Extensive Investigation of Structural, Electronic, Optical, and Thermoelectric Properties of Hybrid Perovskite (Ch3nh3pbbr3) With Mechanical Stability Constants][J]. Energy Weekly News,2020.

[8]. Physics - Applied Physics; Findings on Applied Physics Detailed by Investigators at University of Grenoble-Alpes (An Insight Into the Charge Carriers Transport Properties and Electric Field Distribution of Ch3nh3pbbr3 Thick Single Crystals)[J]. Journal of Physics Research,2020.

[9]. Science - Materials Science; Findings from Kyung Hee University Reveals New Findings on Materials Science (Unique Phonon Modes of a Ch3nh3pbbr3 Hybrid Perovskite Film Without the Influence of Defect Structures: an Attempt Toward a Novel Thz-based Application)[J]. Science Letter,2020.

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4. 毕业设计(论文)计划

2021-1-4~2021-2-24 查阅资料,完成开题报告和外文翻译 2021-2-25~2021-3-10 完成初步论文方案 2021-3-11~2021-4-15 完成放大电路的设计和制作。

2021-4-16~2021-5-20 完成系统的调试和修改。

2021-5-21~2021-6-2 毕业论文撰写,准备答辩

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